【菲羅門氣相手性柱】環氧氯丙烷的手性氣相分離

Epichlorohydrin - chiral separation

Column: FBX-DEX DMT Beta - 0.25mm, 0.25μm, 25m

Conditions:

Oven Program: 40°C isothermal Carrier 

Gas: Hydrogen, 60kPa

Injector: Split, 250°C, split flow 100mL/min, 0.5μL injection volume 

Sample: 1μL (+,-)-Epichlorohydrin in 1mL of Dichloromethane